澆注料是不定形耐火材料的一種，除了具有耐高溫、流動性好、施工方便的特點，還具有抗渣性侵蝕的特點，能夠抵抗酸性和堿性渣的侵蝕，針對不同窯爐內(nèi)襯的耐火材料的侵蝕性，可以選擇針對性的耐火材料，可以有效的勝任其工作，我們來談?wù)劃沧⒘峡乖阅堋?/div>
燒結(jié)富鋁尖晶石的用量控制在基質(zhì)中，剛玉粉和a-Al2O3超微粉末隨電熔融鎂砂粉、鋁酸鹽水泥和SiO2超微粉末的含量變化?？乖囼灢捎蜜釄宸?，1650℃保溫3h，鋼渣采用寶鋼300t轉(zhuǎn)爐終渣。初次裝渣150g，再裝渣130g，循環(huán)試驗。與進口的材料比較，采用剛玉尖晶石耐火澆注料，用于寶鋼300t轉(zhuǎn)爐連鑄鋼包，包齡200次以上。防渣侵透深度為坩堝底與側(cè)壁間侵蝕或滲入的平均深度。
底材對澆注料抗渣性能的影響
不加鎂砂粉和mf-SiO2，水泥用量大，抗渣性差，尤其是熔渣滲透；與編號2和5相比，添加了微量SiO2超微粉，抗渣性略有下降；與編號2和3相比，添加了鎂砂粉，抗熔渣侵蝕性下降，但抗熔渣滲透率卻有增加的趨勢；與編號7相比，添加微量mf-SiO2，抗渣性略有下降。第四號抗渣率與第七號抗渣率相同，號抗渣率與第二號抗渣率也略有下降；第六號抗渣率與第七號進口抗渣率相近。根據(jù)此配方配制成功的低水泥剛玉鎂砂尖晶石質(zhì)耐火澆注料，簡稱為復合鋁鎂尖晶石質(zhì)耐火澆注料。其MgO總含量約為4%，其使用壽命，在300t連鑄剛包上，與進口材料相當或稍高一些。
總之，基體組成對高技術(shù)鋼包耐火澆注料性能的影響是至關(guān)重要的。研究了基質(zhì)組成材料，如鎂砂粉、尖晶石粉、超微粉等對澆注料性能的影響，并確定了佳用量。研制澆注料產(chǎn)品時，應(yīng)合理選擇基質(zhì)組成材料的品種，根據(jù)鋼包的使用和操作條件，材料的化學成分，綜合而適當?shù)卣{(diào)配鎂砂、尖晶石、a-Al2O3和SiO2超微粉的佳配比，以及水泥和外加劑的佳配比，同時加入剛玉粉等高級粉料，以確?；|(zhì)材料的配比占總配比的30%左右。如此在耐火集料品種及級配合理的強力下，才能配制成功，使用性能優(yōu)良的復合鋁鎂尖晶石質(zhì)耐火澆注料，從而保證鋼包的使用壽命。
我們再來介紹一下粘土澆注料
粘結(jié)劑是粘土
耐火澆注料的主要原料之一，也是粘結(jié)劑基材的重要組成部分。粘結(jié)劑的種類和用量對粘結(jié)劑的性能具有重要影響。粘合劑的種類較多，是指一個地方的粘土，由于礦點的不同，其性質(zhì)也有所不同。多年來的試驗和實踐證明，并非所有粘結(jié)粘土都可以作為粘結(jié)劑，只有廣西泥和永吉4號泥較好，其次是焦作泥，像水曲柳這樣的粘土可以勉強使用，但粘結(jié)能力強，需水多，性能差。以下表格是各種粘土對澆注料性能的影響。由表格中可以看出，以廣西泥為粘結(jié)劑，配比的澆注性能佳，其次是焦作泥，其次是水曲柳和巢縣泥，配比性能較差，一般不推薦使用。通過適當選擇粘土結(jié)合劑，可制備出性能優(yōu)良的耐火澆注料。
不同粘性土對澆注料性能的影響
粘結(jié)劑的用量在9%~12%之間。由于粘結(jié)粘土含有較多的低熔點物質(zhì)，耐火性較差，在滿足粘結(jié)粘土耐火性澆注料的工藝要求時，應(yīng)盡量減少其用量。
促凝劑。
粘土巖耐火澆注料促凝劑種類及用量對性能的影響。Ca-70水泥的常溫耐壓強度和高溫耐壓強度均比Ca-50水泥有較好的作用效果，但成本上升幅度較大；3d常溫耐壓強度隨促凝劑用量的增加而增加，高溫時則隨促凝劑用量的增加而降低。
水泥用量對Ca-50澆注料性能的影響
耐火集料
耐火澆注料中，耐火骨料起骨架作用，是澆注料的重要組成部分，占澆注料總量的60%~70%。以下表格是各種耐火集料對澆注料性能的影響。由表格可知，耐火骨料品種按Al2O3含量計算，則隨Al2O3含量的增加，高溫抗壓強度提高，荷重軟化開始溫度提高，4%的變形荷重軟化溫度高于1520℃，三級礬土熟料的荷重軟化溫度略高。為此，以三級礬土熟料作為耐火集料，廣泛應(yīng)用于粘土耐火澆注料中，取得了良好的應(yīng)用效果。
粘土石抗火集料級配，以及抗火集料的品種和細度、含水量及施工條件等因素，對其性能也有一定的影響，與水泥抗火澆注料基本相似，不再贅述；分散劑品種較多，經(jīng)篩選，普遍采用三聚磷酸鈉，分散效果好。
上一篇： 從施工來提高水泥窯耐火材料的使用壽命
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